[1] TOLA M.Occurrence,importance and control of mycotoxins:a review[J].Cogent Food & Agriculture,2016,2(1):1191103.
[2] HUSSEIN H S,BRASEL J M.Toxicity,metabolism,and impact of mycotoxins on humans and animals[J].Toxicology,2001,167(2):101-134.

[3] STOEV S D.Food safety and increasing hazard of mycotoxin occurrence in foods and feeds[J].Critical Reviews in Food Science and Nutrition,2013,53(9):887-901.

[4] OSTRY V,MALIR F,TOMAN J,et al.Mycotoxins as human carcinogens-the IARC monographs classification[J].Mycotoxin Research,2017,33(1):65-73.

[5] ALSHANNAQ A,YU J H.Occurrence,toxicity,and analysis of major mycotoxins in food[J].International Journal of Environmental Research and Public Health,2017,14(6):632.
[6] 丁燕玲,李孟聪,钟名琴,等.2015-2020年国内饲料霉菌毒素污染调查报告统计分析[J].中国动物检疫,2021,38(3):29-36. DING Y L,LI M C,ZHONG M Q,et al.Statistical analysis on the investigation reports concerning mycotoxin contamination in animal feed in China during 2015 to 2020[J].Chinese Journal of Animal Health Inspection,2021,38(3):29-36.(in Chinese)
[7] GRUBER-DORNINGER C,JENKINS T,SCHATZMAYR G.Global mycotoxin occurrence in feed:a ten-year survey[J].Toxins,2019,11(7):375.
[8] WANG Y,LIU N,NING B A,et al.Simultaneous and rapid detection of six different mycotoxins using an immunochip[J].Biosensors & Bioelectronics,2012,34(1):44-50.

[9] SADHASIVAM S,BRITZI M,ZAKIN V,et al.Rapid detection and identification of mycotoxigenic fungi and mycotoxins in stored wheat grain[J].Toxins,2017,9(10):302.
[10] LE V T,VASSEGHIAN Y,DRAGOI E N,et al.A review on graphene-based electrochemical sensor for mycotoxins detection[J].Food and Chemical Toxicology,2021,148:111931.
[11] SINGH J,MEHTA A.Rapid and sensitive detection of mycotoxins by advanced and emerging analytical methods:a review[J].Food Science & Nutrition,2020,8(5):2183-2204.

[12] ZHANG L,DOU X W,ZHANG C,et al.A review of current methods for analysis of mycotoxins in herbal medicines[J].Toxins,2018,10(2):65.
[13] WARTH B,PARICH A,ATEHNKENG J,et al.Quantitation of mycotoxins in food and feed from Burkina Faso and Mozambique using a modern LC-MS/MS multitoxin method[J].Journal of Agricultural and Food Chemistry,2012,60(36):9352-9363.

[14] KOKKONEN M K,JESTOI M N.A multi-compound LC-MS/MS method for the screening of mycotoxins in grains[J].Food Analytical Methods,2009,2(2):128-140.

[15] MONBALIU S,VAN POUCKE C,DETAVERNIER C,et al.Occurrence of mycotoxins in feed as analyzed by a multi-mycotoxin LC-MS/MS method[J].Journal of Agricultural and Food Chemistry,2010,58(1):66-71.

[16] BRYDEN W L.Mycotoxin contamination of the feed supply chain:implications for animal productivity and feed security[J].Animal Feed Science and Technology,2012,173(1/2):134-158.
[17] HE Q H,XU Y,WANG D,et al.Simultaneous multiresidue determination of mycotoxins in cereal samples by polyvinylidene fluoride membrane based dot immunoassay[J].Food Chemistry,2012,134(1):507-512.

[18] REITER E,ZENTEK J,RAZZAZI E.Review on sample preparation strategies and methods used for the analysis of aflatoxins in food and feed[J].Molecular Nutrition & Food Research,2009,53(4):508-524.

[19] ABRUNHOSA L,PATERSON R R M,VENÂNCIO A.Biodegradation of ochratoxin A for food and feed decontamination[J].Toxins,2010,2(5):1078-1099.

[20] KNUTSEN H K,ALEXANDER J,BARREGÅRD L,et al.Risks for animal health related to the presence of zearalenone and its modified forms in feed[J].EFSA Journal.European Food Safety Authority,2017,15(7):e04851.
[21] KNUTSEN H K,ALEXANDER J,BARREGÅRD L,et al.Risks to human and animal health related to the presence of deoxynivalenol and its acetylated and modified forms in food and feed[J].EFSA Journal.European Food Safety Authority,2017,15(9):e04718.
[22] NISHIMWE K,BOWERS E,DE DIEU AYABAGABO J,et al.Assessment of aflatoxin and fumonisin contamination and associated risk factors in feed and feed ingredients in Rwanda[J].Toxins,2019,11(5):270.
[23] 李宇宇,贾玉山,格根图,等.饲用草产品主要真菌毒素污染检测、风险评估与控制研究进展[J].草业学报,2021,30(4):191-204. LI Y Y,JIA Y S,GE G T,et al.Progress in research on detection,risk assessment and control of mycotoxins in forage products[J].Acta Prataculturae Sinica,2021,30(4):191-204.(in Chinese)
[24] DE BAERE S,GOOSSENS J,OSSELAERE A,et al.Quantitative determination of T-2 toxin,HT-2 toxin,deoxynivalenol and deepoxy-deoxynivalenol in animal body fluids using LC-MS/MS detection[J].Journal of Chromatography B:Analytical Technologies in the Biomedical and Life Sciences,2011,879(24):2403-2415.

[25] HOSSAIN M Z,MCCORMICK S P,MARAGOS C M.An imaging surface plasmon resonance biosensor assay for the detection of T-2 toxin and masked T-2 toxin-3-glucoside in wheat[J].Toxins,2018,10(3):119.
[26] IARC.Monographs on the evaluation of carcinogenic risk to humans[M].Lyon:International Agency for Research on Cancer,2002.
[27] 上海飞测生物科技有限公司.黄曲霉毒素的危害、限量标准及检测方法[J].食品安全导刊,2017(13):58-60. Shanghai Feice Biotechnology Co.,Ltd..Hazards of aflatoxin,limit standard and test method[J].China Food Safety Magazine,2017(13):58-60.(in Chinese)
[28] GELINEAU-VAN WAES J,VOSS K A,STEVENS V L,et al.Maternal fumonisin exposure as a risk factor for neural tube defects[J].Advances in Food and Nutrition Research,2009,56:145-181.
[29] 陈茹.国内外饲料真菌毒素限量规定及评析[J].中国饲料,2013(17):38-42. CHEN R.Comparison of domestic and foreign regulation on mycotoxin in feed[J].China Feed,2013(17):38-42.(in Chinese)
[30] European commission.Directive 2002/32 on undesirable substances in animal feed[Z].2010-03-02.
[31] European Commission.Commission recommendation of 17 August 2006 on the presence of deoxynivalenol,zearalenone,ochratoxin A,T-2 and HT-2 and fumonisins in products intended for animal feeding[EB/OL].(2006-08-17)[2021-04-25].https://eur-lex.europa.eu/LexUriServ/LexUriServ.do?uri=OJ:L:2006:229:0007:0009:EN:PDF.
[32] CPG.Sec.683.100 Action levels for alfatoxins in animal feeds[EB/OL].[2021-04-25].https://www.fda.gov/regulatory-information/search-fda-guidance-documents/cpg-sec-683100-action-levels-aflatoxins-animal-feeds.
[33] National Grain and Feed Association.Guidance for industry:fumonisin levels in human foods and animal feeds[EB/OL].(2001-11-09)[2021-04-25].http://feed.ngfa.org/images/uploads/NGFAComplianceGuide-FDARegulatoryGuidanceforMycotoxins8-2011.pdf#:-:text=FDA%20on%20November%209%2C%202001%20issued%20a%20%E2%80%9Cfinal,use%20of%20good%20agricultural%20and%20good%20manufacturing%20practices.%E2%80%9D.
[34] Center for Food Safety and Applied Nutrition,Center for Veterinary Medicine.Guidance for industry and FDA:advisory levels for deoxynivalenol (DON) in finished wheat products for human consumption and grains and grain by-products used for animal feed[EB/OL].(2010-06-29)[2021-04-25].https://www.fda.gov/regulatory-information/search-fda-guidance-documents/guidance-industry-and-fda-advisory-levels-deoxynivalenol-don-finished-wheat-products-human.
[35] 王文珺,孙双艳,叶金,等.我国现行真菌毒素检测标准概述[J].食品安全质量检测学报,2019,10(4):837-847. WANG W J,SUN S Y,YE J,et al.Review of current Chinese of testing standard of mycotoxin[J].Journal of Food Safety & Quality,2019,10(4):837-847.(in Chinese)
[36] 王松雪,鲁沙沙,张艳,等.国内外真菌毒素检测标准制修订现状与进展[J].食品工业科技,2011,32(3):408-412,416. WANG S X,LU S S,ZHANG Y,et al.Current status and advances in the standards of mycotoxin detection[J].Science and Technology of Food Industry,2011,32(3):408-412,416.(in Chinese)
[37] 陈鑫璐,邱月,张建友,等.国内外谷物中多种真菌毒素限量和同步检测标准及方法研究进展[J/OL].中国粮油学报:1-19.(2021-04-21)[2021-04-25].https://kns.cnki.net/kcms/detail/detail.aspx?FileName=ZLYX20210420003&DbName=CAPJ2021. CHEN X L,QIU Y,ZHANG J Y,et al.Domestic and foreign research progress on the limit standards and simultaneous detection standards and methods of multiple mycotoxins in grain[J/OL].Journal of the Chinese Cereals and Oils Association:1-19.(2021-04-21)[2021-04-25].https://kns.cnki.net/kcms/detail/detail.aspx?FileName=ZLYX20210420003&DbName=CAPJ2021.(in Chinese)
[38] 谢瑜杰,陈辉,彭涛,等.食品与饲料基质中真菌毒素检测技术研究进展[J].食品安全质量检测学报,2018,9(6):1234-1246. XIE Y J,CHEN H,PENG T,et al.Research progress on the detection techniques of mycotoxins in food and forage[J].Journal of Food Safety & Quality,2018,9(6):1234-1246.(in Chinese)
[39] ZHANG Z W,HU X F,ZHANG Q,et al.Determination for multiple mycotoxins in agricultural products using HPLC-MS/MS via a multiple antibody immunoaffinity column[J].Journal of Chromatography.B,Analytical Technologies in the Biomedical and Life Sciences,2016,1021:145-152.
[40] ROMERA D,MATEO E M,MATEO-CASTRO R,et al.Determination of multiple mycotoxins in feedstuffs by combined use of UPLC-MS/MS and UPLC-QTOF-MS[J].Food Chemistry,2018,267:140-148.
[41] 薛毅,张玥,吴银良.液相色谱-串联质谱法同时测定饲料中17种霉菌毒素[J].中国畜牧杂志,2016,52(19):90-94. XUE Y,ZHANG Y,WU Y L.Simultaneous determination of seventeen mycotoxins in feeds by liquid chromatography-tandem mass spectrometry[J].Chinese Journal of Animal Science,2016,52(19):90-94.(in Chinese)
[42] CASTEGNARO M,TOZLOVANU M,WILD C,et al.Advantages and drawbacks of immunoaffinity columns in analysis of mycotoxins in food[J].Molecular Nutrition & Food Research,2006,50(6):480-487.

[43] HU X F,HU R,ZHANG Z W,et al.Development of a multiple immunoaffinity column for simultaneous determination of multiple mycotoxins in feeds using UPLC-MS/MS[J].Analytical and Bioanalytical Chemistry,2016,408(22):6027-6036.

[44] 庄倩,曲宝涵,李彦,等.高效液相色谱-串联质谱法同时测定饲料中9种霉菌毒素及其代谢物[J].分析科学学报,2016,32(1):37-42. ZHUANG Q,QU B H,LI Y,et al.Simultaneous determination of nine kinds of mycotoxins and metabolins in feed by high performance liquid chromatography-tandem mass sepectrometry[J].Journal of Analytical Science,2016,32(1):37-42.(in Chinese)
[45] 魏云计,冯民,朱臻怡,等.高效液相色谱-串联质谱法同时测定饲料中11种霉菌毒素[J].色谱,2017,35(8):891-896. WEI Y J,FENG M,ZHU Z Y,et al.Simultaneous determination of 11 mycotoxins in feeds by high performance liquid chromatography-tandem mass spectrometry[J].Chinese Journal of Chromatography,2017,35(8):891-896.(in Chinese)
[46] 张大伟,高和杨,周旌,等.超高效液相色谱-串联质谱法同时检测饲料原料、饲料成品中18种真菌毒素含量[J].食品安全质量检测学报,2018,9(22):5867-5876. ZHANG D W,GAO H Y,ZHOU J,et al.Simultaneous determination of 18 kinds of mycotoxins in feed ingredients and feed products by ultra performance liquid chromatography-tandem mass spectrometry[J].Journal of Food Safety & Quality,2018,9(22):5867-5876.(in Chinese)
[47] 崔晓娜,郭礼强,葛爱民,等.QuEChERS-高效液相色谱-四级杆飞行时间质谱同时测定饲料中17种霉菌毒素[J].江苏农业科学,2018,46(3):177-181. CUI X N,GUO L Q,GE A M,et al.Simultaneous determination of 17 kinds of mycotoxins in feed by QUECHERS-high performance liquid chromatography-quadrupole time-of-flight mass spectrometry[J].Jiangsu Agricultural Sciences,2018,46(3):177-181.(in Chinese)
[48] 苏秋权,殷秋妙,王威利,等.液相色谱串联质谱法同时测定饲料中6种代表性霉菌毒素[J].食品安全质量检测学报,2020,11(15):5142-5149. SU Q Q,YIN Q M,WANG W L,et al.Simultaneous determination of 6 representative mycotoxins in feed by liquid chromatography-tandem mass spectrometry[J].Journal of Food Safety & Quality,2020,11(15):5142-5149.(in Chinese)
[49] 王瑞国,郭丽丽,王培龙,等.杂质吸附型净化结合超高效液相色谱-串联质谱法同时测定谷物和动物饲料中37种霉菌毒素[J].色谱,2020,38(7):817-825. WANG R G,GUO L L,WANG P L,et al.Simultaneous determination of 37 mycotoxins in grain and animal feed by impurity adsorption purification coupled with ultra-performance liquid chromatography-tandem mass spectrometry[J].Chinese Journal of Chromatography,2020,38(7):817-825.(in Chinese)
[50] 范志辰,韩铮,郭文博,等.超高效液相色谱-串联质谱法同时测定不同饲料中30种真菌毒素[J].色谱,2017,35(6):627-633. FAN Z C,HAN Z,GUO W B,et al.Simultaneous determination of 30 mycotoxins in different feed products by ultra high performance liquid chromatography-tandem mass spectrometry[J].Chinese Journal of Chromatography,2017,35(6):627-633.(in Chinese)
[51] 杨立华,翟士星,翟钰,等.液相色谱在食品检测方面的应用[J].食品安全导刊,2017(3):66. YANG L H,ZHAI S X,ZHAI Y,et al.Application of liquid chromatography in food detection[J].China Food Safety Magazine,2017(3):66.(in Chinese)
[52] KONG W J,WEI R W,LOGRIECO A F,et al.Occurrence of toxigenic fungi and determination of mycotoxins by HPLC-FLD in functional foods and spices in China markets[J].Food Chemistry,2014,146:320-326.
[53] 武开业.液相色谱检测器原理及应用[J].科技视界,2014(31):288-288,257. WU K Y.Principle and application of liquid chromatography detector[J].Horizon of Science and Technology,2014(31):288-288,257.(in Chinese)
[54] 刘颖,金永鹏,罗荪琳,等.高效液相色谱同步检测饲料中黄曲霉毒素B
1、玉米赤霉烯酮及呕吐毒素的方法[J/OL].动物营养学报:1-10.(2021-04-20)[2021-05-27].https://kns.cnki.net/kcms/detail/detail.aspx?FileName=DWYX2021041900Z&DbName=CAPJ2021. LIU Y,JIN Y P,LUO S L,et al.A method for simultaneous determination of aflatoxin B
1,zearalenone and deoxynivalenol in feed by high performance liquid chromatography[J/OL].Chinese Journal of Animal Nutrition:1-10.(2021-04-20)[2021-05-27].https://kns.cnki.net/kcms/detail/detail.aspx?FileName=DWYX2021041900Z&DbName=CAPJ2021.(in Chinese)
[55] 朱青欣.液相色谱-质谱联用技术在食品检测中的应用[J].食品安全导刊,2020(20):29-31. ZHU Q X.Application of liquid chromatography-mass spectrometry in food detection[J].China Food Safety Magazine,2020(20):29-31.(in Chinese)
[56] 张钰萍,陈泠竹.液质联用仪及其常用的两种电离源的实验教学[J].当代化工研究,2020(17):114-118. ZHANG Y P,CHEN L Z.Experimental teaching of high performance liquid chromatography/mass spectrometry and two commonly used ionization sources[J].Modern Chemical Research,2020(17):114-118.(in Chinese)
[57] DIANA DI MAVUNGU J,MONBALIU S,SCIPPO M L,et al.LC-MS/MS multi-analyte method for mycotoxin determination in food supplements[J].Food Additives & Contaminants.Part A,Chemistry,Analysis,Control,Exposure & Risk Assessment,2009,26(6):885-895.

[58] RUBERT J,SOLER C,MAÑES J.Application of an HPLC-MS/MS method for mycotoxin analysis in commercial baby foods[J].Food Chemistry,2012,133(1):176-183.

[59] HICKERT S,GERDING J,NCUBE E,et al.A new approach using micro HPLC-MS/MS for multi-mycotoxin analysis in maize samples[J].Mycotoxin Research,2015,31(2):109-115.

[60] JENSEN T,DE BOEVRE M,PREUΒKE N,et al.Evaluation of high-resolution mass spectrometry for the quantitative analysis of mycotoxins in complex feed matrices[J].Toxins,2019,11(9):531.
[61] 符金华,杨琳芬,董泽民,等.饲料和饲料原料等25种样品中16种真菌毒素超高效液相色谱-三重四级杆/线性离子阱串联质谱法基质效应的研究[J].中国饲料,2019(21):66-71. FU J H,YANG L F,DONG Z M,et al.The matrix effect research of determination of 16 mycotoxins by UPLC-quadrupole/Qtrap mass spectrometry in 25 kinds of feed and feedstuff samples[J].China Feed,2019(21):66-71.(in Chinese)
[62] 曾苑,黄少瑶,李仲唐,等.静电场轨道阱质谱技术在食品检测中的发展[J].轻工科技,2019,35(3):4-6,9 ZENG Y,HUANG S Y,LI Z T,et al.Development of electrostatic field orbitrap mass spectrometry technology in food inspection[J].Light Industry Science and Technology,2019,35(3):4-6,9.(in Chinese)
[63] 陈瑞鹏,孙云凤,霍冰洋,等.真菌毒素多重检测技术的研究进展[J/OL].食品科学:1-11.(2020-12-03)[2021-05-27].https://kns.cnki.net/kcms/detail/detail.aspx?FileName=SPKX2020112000H&DbName=CAPJ2020. CHEN R P,SUN Y F,HUO B Y,et al.Research progress of multiple detection technology of mycotoxins[J/OL].Food Science:1-11.(2020-12-03)[2021-05-27].https://kns.cnki.net/kcms/detail/detail.aspx?FileName=SPKX2020112000H&DbName=CAPJ2020.(in Chinese)